TA Instruments

AR1754-0002f

15/03/2013 14:10:59

Sample name	ASW Blank coupon#24 + P120 
Sample notes	 
Experiment notes	ASW Articial Sea Water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1754
Run number	2 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 14:10:59

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	299.9	-196.78	10000	20.0	-0.07223	3.004	-64.14	374.9	-0.1711	-294.3	250.4580	-2.094E-3	313.07	31307	3.411E-3	0.0	0.1
2.0040	300.0	951.23	10000	20.0	-0.1424	4.004	310.1	375.0	0.8269	-580.3	500.9740	-4.127E-3	626.22	62622	3.411E-3	0.0	0.1
3.0040	300.0	930.13	10000	20.0	-0.1599	5.004	303.2	375.0	0.8085	-651.4	876.4500	-4.632E-3	1095.6	1.0956E5	3.411E-3	0.1	0.1
4.0160	300.0	904.82	10000	20.0	-0.1459	6.016	294.9	375.0	0.7864	-594.4	1127.7400	-4.226E-3	1409.7	1.4097E5	3.411E-3	0.1	0.1
5.0040	300.0	913.70	10000	20.0	-0.1485	7.004	297.8	375.0	0.7942	-605.1	1381.2500	-4.303E-3	1726.6	1.7266E5	3.411E-3	0.1	0.1
6.0160	300.0	889.58	10000	20.0	-0.1530	8.016	290.0	375.0	0.7733	-623.3	1755.9700	-4.433E-3	2195.0	2.1950E5	3.411E-3	0.1	0.1
7.0040	300.0	887.59	10000	20.0	-0.1445	9.004	289.3	375.0	0.7715	-588.6	2009.1700	-4.185E-3	2511.5	2.5115E5	3.411E-3	0.1	0.2
8.0080	300.0	888.69	10000	20.0	-0.1501	10.008	289.7	375.0	0.7724	-611.7	2384.2600	-4.350E-3	2980.3	2.9803E5	3.411E-3	0.1	0.2
9.0200	300.0	896.99	10000	20.0	-0.1422	11.020	292.4	375.0	0.7797	-579.5	2635.7200	-4.121E-3	3294.7	3.2947E5	3.411E-3	0.2	0.2
10.004	300.0	904.05	10000	20.0	-0.1428	12.004	294.7	375.0	0.7858	-582.0	2888.2600	-4.139E-3	3610.3	3.6103E5	3.411E-3	0.2	0.2
11.004	300.0	895.22	10000	20.0	-0.1532	13.004	291.8	375.0	0.7781	-624.1	3263.8601	-4.438E-3	4079.8	4.0798E5	3.411E-3	0.2	0.2
12.016	300.0	887.86	10000	20.0	-0.1503	14.016	289.4	375.0	0.7717	-612.5	3516.6201	-4.355E-3	4395.8	4.3958E5	3.411E-3	0.2	0.2
13.004	300.0	895.70	10000	20.0	-0.1487	15.004	292.0	375.0	0.7785	-605.9	3894.5701	-4.309E-3	4868.2	4.8682E5	3.411E-3	0.2	0.3
14.004	300.0	885.14	10000	20.0	-0.1554	16.004	288.5	375.0	0.7694	-633.2	4143.6699	-4.503E-3	5179.6	5.1796E5	3.411E-3	0.2	0.3
15.004	300.0	881.20	10000	20.0	-0.1581	17.004	287.2	375.0	0.7659	-644.0	4395.8999	-4.579E-3	5494.9	5.4949E5	3.411E-3	0.3	0.3
16.004	300.0	896.45	10000	20.0	-0.1578	18.004	292.2	375.0	0.7792	-643.1	4774.4702	-4.574E-3	5968.1	5.9681E5	3.411E-3	0.3	0.3
17.004	300.0	892.21	10000	20.0	-0.1483	19.004	290.8	375.0	0.7755	-604.3	5029.2500	-4.297E-3	6286.6	6.2866E5	3.411E-3	0.3	0.3
18.016	300.0	870.14	10000	20.0	-0.1625	20.016	283.6	375.1	0.7562	-662.1	5274.4800	-4.707E-3	6593.1	6.5931E5	3.411E-3	0.3	0.3
19.016	300.0	882.60	10000	20.0	-0.1548	21.016	287.7	375.0	0.7672	-630.7	5652.8301	-4.485E-3	7066.0	7.0660E5	3.411E-3	0.3	0.4
20.016	300.0	885.00	10000	20.0	-0.1451	22.016	288.5	375.0	0.7692	-591.1	5904.2402	-4.203E-3	7380.3	7.3803E5	3.411E-3	0.3	0.4
21.004	300.0	898.38	10000	20.0	-0.1414	23.004	292.8	375.0	0.7810	-576.2	6282.2002	-4.098E-3	7852.8	7.8528E5	3.411E-3	0.4	0.4
22.004	300.0	880.05	10000	20.0	-0.1587	24.004	286.9	375.0	0.7650	-646.4	6533.7202	-4.597E-3	8167.2	8.1672E5	3.411E-3	0.4	0.4
23.016	300.0	873.66	10000	20.0	-0.1447	25.016	284.8	375.0	0.7594	-589.4	6782.6499	-4.191E-3	8478.3	8.4783E5	3.411E-3	0.4	0.4
24.004	300.0	877.92	10000	20.0	-0.1512	26.004	286.2	375.0	0.7630	-615.9	7161.8599	-4.379E-3	8952.3	8.9523E5	3.411E-3	0.4	0.4
25.004	300.0	878.90	10000	20.0	-0.1522	27.004	286.5	375.0	0.7639	-620.0	7417.9600	-4.409E-3	9272.5	9.2725E5	3.411E-3	0.4	0.5
26.008	300.0	885.09	10000	20.0	-0.1550	28.008	288.5	375.0	0.7693	-631.6	7787.9600	-4.491E-3	9735.0	9.7350E5	3.411E-3	0.4	0.5
27.020	300.0	888.89	10000	20.0	-0.1479	29.020	289.7	375.0	0.7727	-602.6	8039.4399	-4.286E-3	10049	1.0049E6	3.411E-3	0.5	0.5
28.016	300.0	887.94	10000	20.0	-0.1512	30.016	289.4	375.0	0.7718	-615.9	8290.6504	-4.380E-3	10363	1.0363E6	3.411E-3	0.5	0.5
29.004	300.0	870.68	10000	20.0	-0.1483	31.004	283.8	375.0	0.7567	-604.3	8670.4199	-4.296E-3	10838	1.0838E6	3.411E-3	0.5	0.5
30.016	300.0	889.77	10000	20.0	-0.1495	32.016	290.0	375.0	0.7733	-609.2	8918.9404	-4.332E-3	11149	1.1149E6	3.411E-3	0.5	0.5

